The method is suitable for the determination of water vapor volatile aroma compounds in beer.
Volatile aroma compounds are driven out of the sample through steam distillation. The ethanolic distillate is saturated with NaCl. Potassium hydrogen sulfite is added to separate carbonyl groups that might interfere with the analysis. The extraction of the aroma compounds is performed by shaking out with dichloromethane and the phases separated by centrifuging.
The method is suitable for beer brewed to any original gravity or to any alcohol content.
Volatile compounds in beer are concentrated through distillation and extracted with dichloromethane. The solvent phase is analyzed with a gas chromatograph. The linearity of the detector and the determination of the concentrations of analytes in the sample are achieved by using multiple concentration levels within the relevant range and through evaluation of the relative area under the peaks.
Determination of organic acids by means of reversed phase chromatography/ion chromatography
This method is suitable for wine, fruit juice and other non-alcoholic beverages.
The organic acids are separated using two combined columns, reversed-phase HPLC and an ion exchange column and are then determined using a UV detector.
This method describes how to determine the acid consumption or acid capacity of water.
Water intended for use as an ingredient in the production of beer (brewing liquor) or other foods
This method describes how to determine the moisture content of specialty malt.
Specialty malt intended for use in beer brewing or elsewhere in the food industry
The method is suitable for beers of all original gravities and of any alcohol content.
The gas chromatography headspace method is used to determine the higher alcohols and esters present in beer, i.e., the volatile compounds are transferred from the headspace in the sample vial into the GC system for analysis. The following substances are measured in this analysis:
Acetaldehyde
Propanol-1
Ethyl acetate
2-Methylpropanol
3-Methylbutanol
2-Methylbutanol
2-Methylpropylacetate
Butyric acid ethyl ester
3-Methylbutyl acetate
2-Methylbutyl acetate
Hexanoic acid ethyl ester