Water intended for use as an ingredient in the production of beer (brewing liquor) or other foods
Determination of the dry residue (ash content) of a filtered or unfiltered water sample.
Water intended for use as an ingredient in the production of beer (brewing liquor) or other foods
A specified quantity of water is evaporated, and any remaining moisture is subsequently eliminated in a drying oven. The dry residue is then weighed.
Suitable for analysis of all (laboratory) wort samples
Copper in wort is measured using AAS by directly aspirating the diluted sample into an air-acetylene flame or by electrothermal atomization; the measurement is made at 324.7 nm.
Wastewater generated in the industrial production of beer and food
Well-mixed wastewater is poured into an Imhoff funnel, and the volume of sludge is recorded using the volumetric scale on the graduated cylinder after a settling time of two hours.
After decanting the supernatant, the deposits are quantitatively transferred to a platinum dish in which, after drying at 105 °C, the dry residue after evaporation is determined by weight.
After annealing in a muffle furnace at 550 °C for 30 min, the ash content is determined gravimetrically.
The annealing losses are calculated from the difference in weight between the dry residue after evaporation and the ash content.
Determination of the fermentation cellar yield in order to monitor brewhouse operations
Wort from the midpoint of chilling/pitching wort
The fermentation cellar yield is calculated using the value determined for the amount of extract contained in a batch of wort relative to the amount of extract present in the raw materials used to produce the wort.
The gelatinization temperature can be determined using a rotary viscometer (e.g., Amylograph or Viscograph, Brabender GmbH & Co. KG, Germany [4] or a Rapid-Visco-Analyser, RVA, Perten Instruments, a PerkinElmer Company, USA [8]).
A suspension consisting of a finely ground sample and water is produced, whose precise mixing ratio should correspond to the analysis protocol for the adjunct in question. However, since for many cereals and pseudocereals no official analysis protocol exists, the initial weight for the adjuncts listed in table 2 has been determined empirically [3].
Once the suspension is prepared it is attempered according to a pre-programmed temperature/time program, and the viscosity is determined on a continuous basis by means of a rotor and a rotary torque measurement (fig. 1). When gelatinization begins, an increase in the viscosity is registered, and the corresponding sample temperature is defined as the gelatinization temperature. The standard evaluation criterion (PT) is a viscosity increase of at least 24 cP (≙ mPas) within six seconds.