The method describes the appropriate procedure for sample collection of adjuncts, barley and malt.
Material, which is intended for processing in a food production facility, must be sampled prior to or at the time of delivery.
Malt intended for use in beer brewing or elsewhere in the food industry
Viscometric Determination of Gelatinization Temperature (GT)
The gelatinization temperature (GT) can be determined using a rotary viscometer (e.g., amylograph or viscograph, Brabender GmbH & Co. KG, Germany [7] or Rapid-Visco-Analyser (RVA), Perten Instruments, a PerkinElmer Company, USA [8]).
Unlike the analysis method for adjuncts which do not contain a large amount of enzymes, for the analysis of barley malt, a mash with a mash to sparge ratio of 1 : 4 (similar to that commonly found in the brewing process) is used [9]. The sample is heated according to a programmable temperature/time program (refer to table 1) and the viscosity is measured using measuring stirrer throughout the process.
A gelatinization begins to occur, an increase in viscosity is registered; temperature of the sample is measured and identified as the corresponding gelatinization temperature. An increase in viscosity of a minimum of 24 cP (mPa × s) within six seconds is the evaluation criterion for the pasting temperature.
This method describes how to determine the moisture content of specialty malt.
Specialty malt intended for use in beer brewing or elsewhere in the food industry
This method describes how to correctly collect a sample of water.
Water intended for use as an ingredient in the production of beer (brewing liquor) or other foods
Collecting samples correctly is a prerequisite for obtaining flawless analytical results. The sample collection method must be adapted to align with the purpose of the analysis method. As a rule, separate samples are taken for chemical and microbiological analyses, since different equipment and containers are required for the collection and treatment of samples.
In principle, sample collection methods are distinguished as follows:
Random samples collected for analysis identify possible contamination or can be collected for purposes of orientation prior to more extensive sampling.
Both intermittent (discontinuous) sample collection (according to certain time intervals, volumes or flow rates) and continuous sampling, which allows for constant monitoring of flowing water for compliance with quality standards, are possible. Samples taken continuously can be mixed to create composite samples and provide mean data.
A series of samples (taken at different depths or over a given area to perform profile tests) are collected for analysis in the process of testing standing water.
Determination of the fermentation cellar yield in order to monitor brewhouse operations
Wort from the midpoint of chilling/pitching wort
The fermentation cellar yield is calculated using the value determined for the amount of extract contained in a batch of wort relative to the amount of extract present in the raw materials used to produce the wort.
This method describes how to determine whether kernels are cracked as part of the visual and manual inspection of a lot of barley.
Barley intended for the production of malt is to be evaluated on the basis of the characteristics described below.
Visual assessment