This method describes how the extract content of adjuncts is determined.
After gelatinization of the starch in the adjunct, the starch is liquefied and converted through the addition of malt. Subsequently, the extract content is determined according to the procedure given in the method for malt analysis.
The nitrogen/raw protein content of barley intended for the production of brewing malt must be determined in advance.
The sample is combusted in a pure oxygen atmosphere at approx. 1000 °C. The resulting mix of gases comes into contact with a CuO/Pt catalyst and is thereby completely oxidized and subsequently freed of all by-products which could potentially interfere with analysis.
After the nitrogen oxides formed in the combustion process are reduced upon contact with tungsten, all nitrogen compounds in the sample are reduced to elemental nitrogen (N2). The elemental nitrogen is then detected by means of a thermal conductivity detector (TCD), the signal of which is quantitatively evaluated by a dedicated integrator.
This method describes how to determine the extract content of liquid adjuncts by means of relative density measurement.
Adjuncts in liquid form which are soluble in water
Determination of relative density sL 20/20 °C with a pycnometer or other suitable density measurement device
Hop extract intended for use in beer brewing or elsewhere in the food industry
SO2 in the Karl Fischer solution creates an ester with methanol, which is neutralized through a reaction with a base. The anions of methylated sulfuric acid are the reactive component in the chemical reaction. In the water titration, the methyl sulfite anions are oxidized by iodine to form methyl sulfate. The endpoint can be determined either by a color change (addition of a starch solution) or electrochemically.
This method describes how to determine the total nitrogen content by means of the combustion method according to Dumas.
Malt intended for use in beer brewing or elsewhere in the food industry.
Suitable for all (laboratory) worts
Wort is produced using a laboratory mash method (fine grind) after which the nitrogen content of the wort is determined.